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Electrochemical determination of chloramphenicol using a glassy carbon electrode modified with dendrite-like Fe₃O₄ nanoparticles
Krishnan Giribabu, Sung-Chan Jang, Yuvaraj Haldorai, Muruganantham Rethinasabapathy, Seo Yeong Oh, Arunkumar Rengaraj, Young-Kyu Han 한국탄소학회 Carbon Letters 10 Pages
한국탄소학회 Carbon Letters 2017, Vol.23 6 38-47 (10 pages)
In this study, magnetite (Fe3O4) nanoparticles were electrochemically synthesized in an aqueous electrolyte at a given potential of -1.3 V for 180 s. Scanning electron microscopy revealed that dendrite-like Fe3O4 nanoparticles with a mean size of < 80 nm were electrodeposited on a glassy carbon electrode (GCE). The Fe3O4/GCE was utilized for sensing chloramphenicol (CAP) by cyclic voltammetry and square wave voltammetry. A reduction peak of CAP at the Fe3O4/GCE was observed at 0.62 V, whereas... -
Synthesis and characterization of carbon doped TiO₂ photocatalysts supported on stainless steel mesh by sol-gel method
JO. Tijani, OO. Fatoba, TC. Totito, WD. Roos, LF. Petrik 한국탄소학회 Carbon Letters 12 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 6 48-59 (12 pages)
This study synthesized pure anatase carbon doped TiO₂ photocatalysts supported on a stainless steel mesh using a sol-gel solution of 8% polyacrylonitrile (PAN)/dimethylformamide (DMF)/TiCl₄. The influence of the pyrolysis temperature and holding time on the morphological characteristics, particle sizes and surface area of the prepared catalyst was investigated. The prepared catalysts were characterized by several analytical methods: high resolution scanning electron microscopy (HRSEM), energy... -
Three-dimensional porous graphene materials for environmental applications
Muruganantham Rethinasabapathy, Sung-Min Kang, Sung-Chan Jang, Yun Suk Huh 한국탄소학회 Carbon Letters 13 Pages
한국탄소학회 Carbon Letters 2017, Vol.22 1 1-13 (13 pages)
Porous materials play a vital role in science and technology. The ability to control their pore structures at the atomic, molecular, and nanometer scales enable interactions with atoms, ions and molecules to occur throughout the bulk of the material, for practical applications. Three-dimensional (3D) porous carbon-based materials (e.g., graphene aerogels/hydrogels, sponges and foams) made of graphene or graphene oxide-based networks have attracted considerable attention because they offer low... -
Functionalization of graphene nanoplatelets using sugar azide for graphene/epoxy nanocomposites
Saswata Bose, Lawrence T. Drzal 한국탄소학회 Carbon Letters 6 Pages
한국탄소학회 Carbon Letters 2015, Vol.16 No.2 5 101-106 (6 pages)
We report a covalent functionalization of graphene nanoparticles (GnPs) employing 2,3,4-Tri-O-acetyl-β-D-xylopyranosyl azide followed by fabrication of an epoxy/functionalized graphene nanocomposite and an evaluation of its thermo-mechanical performance. Successful functionalization of GnP was confirmed via thermal and spectroscopic study. Raman spectroscopy indicated that the functionalization was on the edge of the graphene sheets; the basal plane was not perturbed as a result of the... -
Hierarchical porous carbon nanofibers via electrospinning
Aikifa Raza, Jiaqi Wang, Shan Yang, Yang Si, Bin Ding 한국탄소학회 Carbon Letters 14 Pages
한국탄소학회 Carbon Letters 2014, Vol.15 No.1 1 1-14 (14 pages)
Carbon nanofibers (CNFs) with diameters in the submicron and nanometer range exhibit high specific surface area, hierarchically porous structure, flexibility, and super strength which allow them to be used in the electrode materials of energy storage devices, and as hybrid-type filler in carbon fiber reinforced plastics and bone tissue scaffold. Unlike catalytic synthesis and other methods, electrospinning of various polymeric precursors followed by stabilization and carbonization has become a... -
금나노 물질이 북방산개구리에 미치는 영향
김은지, 고원배, 한얼, 김호진, 고정원, 정훈 한국습지학회 한국습지학회지 7 Pages
한국습지학회 한국습지학회지 2015, Vol.17 No.4 10 407-413 (7 pages)
나노물질이 포함된 다양한 제품들이 증가하고 있으며, 나노물질의 수생태계 노출에 대해서는 불가피하다. 따라서 우리 는 금나노입자를 이용하여 국내 다양한 습지 환경에 널리 서식하는 북방산개구리에 대한 독성평가(부화율, 바디컨디 션, 행동학적민감도)를 해보았다. 행동학적 민감도는 포식자 회피반응 정도를 이용하여 Ethvision XT 9으로 측정하였 다. 금나노입자에 대한 부화율과 STL의 독성은 나타나지 않았다. 하지만 금나노입자에 노출된 올챙이들은 외부자극에 대한 행동학적 민감도가 감소하였다. 이러한 결과는 실험대상... -
광화학적 반응을 이용한 편극 패턴된 강유전체 표면에 금속 나노입자의 증착에 관한 연구
박영식, 김정훈, 양우철, Park. Young-Sik, Kim. Jung-Hoon, Yang. Woo-Chul 한국진공학회 韓國眞空學會誌 7 Pages
한국진공학회 韓國眞空學會誌 2011, Vol.20 No.4 300-306 (7 pages)
PPLN의 각 영역의 편극 방향은 Piezoresponse force microscopy로 확인하였다. 금속(Ag, Au) 나노 입자는 금속이 포함된 수용액에 PPLN 기판을 넣고, 자외선 램프로 30초에서 3분간 노출시켜 광환원 반응으로 기판에 증착시켰다. 시료 성장후, 공기 중에서 AFM을 이용하여 나노입자의 형태, 크기, 및 표면분포를 조사하였다. Ag 입자의 경우, -Z 편극 영역보다 +Z 편극 영역에 크고 밀도가 높은 나노 입자가 증착되었으며, 특히 편극 경계 부분에 가장 큰 Ag 나노입자가 증착되어, 나노선 모양으로 성장됨이 확인되었다. 그러나 Au 입자의...


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