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습식화학 방법에 의한 안정화된 $ZrO_2$의 제조 및 특성에 대한 연구
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  • 습식화학 방법에 의한 안정화된 $ZrO_2$의 제조 및 특성에 대한 연구
저자명
전승범,변수일
간행물명
요업학회지
권/호정보
1979년|16권 3호|pp.155-163 (9 pages)
발행정보
한국세라믹학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

This study was to explore the characteristics of 6 mole% CaO stabilized $ZrO_2$ prepared by wet chemical methods. The results of the experiments were as follows: 1. The powder calcined at 1000$^{circ}$-110$0^{circ}C$ was partly agglomerated. The morphology of agglomerate was spherical of 0.5-1$mu{m}$ in size for Hot Petroleum Drying Method, chain-like of 1-2$mu{m}$ for Freeze Drying Method, and irreqular of 2-3$mu{m}$ for Coprecipitation Method. 2. Optimum calcining conditions for powder prepared by wet chemical methods were found: 110$0^{circ}C$, 2h in air for Hot Petroleum Drying Method and Freeze Drying Method, and 100$0^{circ}C$, 2h in air for Coprecipitation Method. 3. When specimen was calcined at 1000$^{circ}$-110$0^{circ}C$ in air for 2h and then sintered at 1$600^{circ}C$ in air for 4h, the specimens prepared by wet chemical methods showed a high sintered density (94% of theoretical density) and a low open porosity (<0.8%); however, the sintered density of the specimen prepared by Oxide Wet Mixing Method was 90%. 4. The amount of cubic phase of sintered body prepared by wet chemical methods was observed to be higher than the one prepared by Oxide Wet Mixing Method. 5. It was found that Hot petroleum Drying Method, Freeze Drying Method and Coprecipitation Method were nearly the same in respect of the results of stabilization grade and sintered density of CaO-stabilized $ZrO_2$.