- 습식법으로 제조한 수산화아파타이트 분말의 소결과 그 미세구조에 미치는 Ca/P몰비의 영향
- ㆍ 저자명
- 신용규,정형진,김병호
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1989년|26권 1호|pp.123-131 (9 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Hydroxyapatite powders were syntehsized by the reaction of Ca(NO3)2.4H2O and (NH4)2HPO4 in aqueous solution. The effect of the Ca/P mole ratio in the starting solution on the sintering of the powders and its microstructure was studied. When the Ca/P mole ratio in the starting solution was 1.69, the relative density of the sintered bodies was more than 95%. The sinterability was decreased as the Ca/P mole ratio in the starting solution was increased (Ca/P mole ratio >1.67). Hydroxyapatite sintered bodies obtained from the Ca/P mole ratio=1.69 had very excellent bending strength. The best bending strength was obtained at 110$0^{circ}C$ and its value was 1220kg/$ extrm{cm}^2$. The average grain size was 0.277${mu}{ extrm}{m}$. Most of sintered bodies were almost shown 100% hydroxyapatite phase. However, in case of the Ca/P mole ratio=1.64 hydroxyapatite was decomposed to $alpha$-whitlockite above 120$0^{circ}C$.