On this study. Constructed the system detecting the reflective acoustic waves from the solid-samples using the 3MHZ focused-acoustic transducer and detected the V(Z) charateristics curves varied by the distance between the focusing position and the solid surface. The results of the experimental detection to various solid materials showed that the materials have their own unique shape of V(Z) curves. This paper suggested the possibility distinguishing the solid characteristics by analysing the V (Z) curves.