The purpose of this study is to develop the non-destructive material evaluation method of aluminum alloy base metal matrix composite(MMC) by ultrasonics. Five aluminum base MMC specimens were fabricated in which the fractional ratios of fiber were changed from 0% to 31%. Relations among acoustic properties, microstructural features and elastic constant were compared. The ultrasonic velocity method was useful for nondestructive elastic constant measurement of composite materials, since the method had as same accuracy as conventional strain measurement method. Furthermore, velocity, attenuation and backscattering behaviors for each specimen also related to fractional ratio of fiber and these relations could utilize ultrasonic non-destructive evaluation of fiber structure in MMC.