In this research a novel two-reference-beam double pulse holographic technique for the measurments of particle sizes and velocities was developed. This holographic method features the capability of separation of the first and second particle images by using two reference beams instead of one and the change of the polarization direction of laser light. The developed holographic system was tested through the measurements of droplet sizes and velocities in the spray created by two high speed impinging jets. The overall spray pattern clearly revealed the inherent wave nature. Smaller and faster droplets were generated with larger impingement angle, higher jet velocity. and smaller orifice diameter.