- PbO-TiO$_2$-B$_2$O$_3$-BaO 계 유리에서 PbTiO$_3$ 결정의 핵생성 곡선 결정을 위한 열시차분석법의 응용
- ㆍ 저자명
- 이선우,심광보,오근호
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1998년|35권 6호|pp.640-646 (7 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Nucleation and crystallzation of a quaternary glass system for lead titanate glass-ceramics were in-vestigated using DTA(differential thermal analysis ) with variation of nucleation temperature and crystal growth time. Glass samples containing 60mol% of PbO-{{{{ { TiO}_{2 } }} were prepared from melts by the conventional normal cooling method in a cylindrical brass mould. The glass sample was nucleated between 40$0^{circ}C$ and 50$0^{circ}C$ for a given time and showed the maximum nucleation rate at 46$0^{circ}C$ The DTA crystallization peak temperature decreased with increasing nucleating time and decreasing heating rate during DTA runs which indicated an increase of the number of nuclei produced in the system