This paper presents the results of the first interlaboratory comparison of ambient particles measurement conducted by 5 laboratories under the framework of Korean Society for Atmospheric Environment(KOSAE) on the May of 1998 in Seoul. Collection of particles less than 10$mu extrm{m}$(PM10) was carried out by two different types of PM10 sampler, and their concentration reported by three laboratories ranged from 36.2~56.05$mu extrm{g}$/㎥. Analyses of chemical composition of particles collected by each lab were performed by the destructive and nondestructive instrumental methods. Statistical analysis of the measurement results could not be carried out because a comprehensive QA/QC had not been applied before experiment. The importance of QA/QC as well as the performance of QA/QC for the measurement of PM10 was discussed in detail.