- 미세구조 제어에 의해 제조한 자체 강인화 질화규소 세라믹의 기계적 성질과 미세조직
- ㆍ 저자명
- 김완중,이영규,조원승,최상욱
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1999년|36권 4호|pp.432-443 (12 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
The self-toughened Si3N4 ceramics where needle-like coarse ${eta}$-Si3N4 grains were dispersed within fine-grain-ed matrix were prepared via hot-prssing at 1730$^{circ}C$ for 2 h using 5 vol% ${eta}$-Si3N4 whiskers as a seed. In this study the microstructures and mechanical properties of self-toughened Si3N4 ceramics were investigated. The flexural strength of self-toughened Si3N4 ceramics was increased from 600-800 MPa of the Si3N4 monolith to 830-1025 MPa. The KIC was also increased from 4.0-5.0MPa$.$m1/2 of the Si3N4 monolith to 5.8-6.5MPa$.$m1/2$.$The needle-like coarse Si3N4 grains in self-toughened ceramics were considered to induce various toughening mechanisms including the crack deflection pull-out and bridging and to contribute to KIC improvement. In ad-dition to toughening mechanisms the KIC improvement was considered to be partially indebted also to the orien-tation of large ${eta}$-Si3N4 grains and to the promoting effect of ${eta}$-Si3N4 whiskers on the ${alpha}$ to ${eta}$ transtion.