- 상압소결에 의해 제조한 자체 강인화 질화규소 세리믹의 미세조직과 기계적 성질
- ㆍ 저자명
- 김완중,이영규,조원승,최상욱
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1999년|36권 5호|pp.547-554 (8 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
The self-reinforced Si3N4 ceramics were prepared by pressureless-sintering using ${eta}$-Si3N4 whiskers as a seed. Effects of ${eta}$-Si3N4 whiskers on microstructure and mechanical properties and the ${alpha}$ to ${eta}$ phase transition of Si3N4 were investigated. The self-reinforced Si3N4 ceramics were densified(relative density$geq$98%) by pressureless-sintering (1800$^{circ}C$ 2h) using 8mol% Y2O3 and 6mol% Al2O3 as sintering aids and 5 vol% ${eta}$-Si3N4 whiskers within self-reinforced Si3N4 ceramic seemed to hinder the densification owing to their acicular shapes but accelerated the ${alpha}$ to ${eta}$ phase transition because they acted as pre-existing nuclei. It was found that the more ${eta}$-Si3N4 nucei the faster ${alpha}$ to ${eta}$ phase transition.