A three-dimensional digital image processing technique is proposed to quantitatively predict the dispersion phenomena of oil droplet onto the surface of the water. This technique is able to get the dispersion rate of an oil droplet three-dimensionally just below the surface of the water over time. The obtained dispersion rate obtained through this technique is informative to the investigation into the relationship among the gravity, surface tensions between oil, water, and air. This technique is based upon the three-dimensional PIV(Particle Imaging Velocimetry) technique and its system mainly consists of a three CCD(Charge Coupled Device) cameras, an image grabber, and a host computer in which an image processing algorithm is adopted for the acquisition of dispersion rate oil an oil droplet.