- 수열합성 법에 의한 $BaTiO_3$ 분말제조 및 방전 플라즈마 소결
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- 한국분말야금학회지
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- 2001년|8권 1호|pp.35-41 (7 pages)
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- 한국분말야금학회
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$BaTiO_3$ fine powder was synthesized by hydrothermal process from the mixture of titania-hydroxide($TiO_2{cdot}xH_2O$) and barium hexa-hydroxide ($Ba(OH)_2{cdot}8H_2O$) as starting materials. Fine powder(< 100 nm) was made under the reaction conditions of 18$0^{circ}C$,10 atm, 1.5 hr in autoclave and showed cubic structure. The powders were sintered by a spark plasma sintering technique from 1050~115$0^{circ}C$ for 5 min. The grains of sample sintered at 110$0^{circ}C$ were about 0.9${mu}m$ in average size and showed the mixture of cubic and tetragonal structures.