The SCM420 used mainly to automobile transmission gear has problems that it costs transmission gear maker much money in carburising treatment. For this, it needs to alternate the existing material and heat treatment to new gear material and surface modification. For this, friction and wear experiment according to sliding speed and applied load was carried out to evaluate the wear resistance of two transmission gear materials with carburising SCM420 and nitrocarburising NT100, The presumed wear volume was calculated with the image processing for evaluation of wear resistance of two transmission gear materials. The results show that nitrocarburising NT100 has a distinguished wear resistance than carburising SCM420.