- 식용란중 벤지미다졸계 구충제 분석
- ㆍ 저자명
- 강형주,김문배,이재봉,김봉식,김영갑,Kang. Hyung-Joo,Kim. Mun-Bae,Lee. Jae-Bong,Kim. Bong-Sik,Kim. Young-Kab
- ㆍ 간행물명
- 韓國家畜衛生學會誌
- ㆍ 권/호정보
- 2003년|26권 2호|pp.157-162 (6 pages)
- ㆍ 발행정보
- 한국가축위생학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
This stud was attempted to detect six benzimidazoles[thiabendazole(TBZ), oxfendazole(OFZ), mebendazole(MBZ), flubendazole(FLBZ), albendazole(ABZ), and febendazole(FBZ)] in eggs using high performance liquid chromatography(HPLC) with photodiode array detector(DAD) simultaneously. The eluates were determined by HPLC on a waters X-Terra$^{TM};C_{18}$ reverse-phase column($4.6{ imes}250nm,;5{mu}m$) with DAD at 295nm. The mobile phase was 0.04M ammonium phosphate(pH 7.5)/ACN(62.28 v/v) run isocratically. The calibration curves were linear(r>0.999) for six benzimidazoles. Average recovery rate from eggs were 94.54% for TBZ, 97.71% for OFZ, 88.82% for MBZ, 93.71% for FLBZ, 78.61% for ABZ, and 75.09% for FBZ, respectively. The limits of detection and quantification were 2.27ppb, 3.88 for TBZ, 9.34ppb, 15.61ppb for OFZ, 28.53ppb, 45.15ppb for MBZ, 27.39ppb, 40.95ppb for FBZ, 8.61ppb, 13.95ppb for ABZ and 12.79ppb, 22.34ppb for FBZ, respectively.