Two-dimensional laser visualization methods have been used in the study of breakup and atomization processes of non-evaporating diesel sprays. A single-hole spray injected into a quiescent atmospheric environment was visualized by the LIF(Laser Induced Fluorescence) and scattering technique. The LIF technique could be implemented to take the images which are magnified enough to show the shape of liquid ligaments and small droplets. The spontaneous scattering and fluorescent images of sprays were also taken to investigate the atomization of droplets. In the tip and periphery of a spray. the scattering light is bright and the ratio of fluorescent/scattering intensity is lower. This characteristics indicate the very high number density of small droplets which are well atomized.