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기계적 분쇄화 및 스파크 플라즈마 소결에 의한 TiAl 합금의 제조
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  • 기계적 분쇄화 및 스파크 플라즈마 소결에 의한 TiAl 합금의 제조
저자명
김민수,김준식,황승준,홍영환,오명훈,Kim. M.S.,Kim. J.S.,Hwang. S.J.,Hong. Y.H.,Oh. M.H.
간행물명
열처리공학회지
권/호정보
2004년|17권 1호|pp.17-22 (6 pages)
발행정보
한국열처리공학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

In the present study, newly developed spark plasma sintering(SPS) technique was introduced to refine the grain size of ${gamma}$-based TiAl intermetallic compounds. Ti-46Al-1.5Mo and Ti-46Al-1.5Mo-0.2C(at%) prealloyed powders were produced by mechanical milling(MM) in high-energy attritor. The mechanically milled powders were characterized by XRD and SEM for the microstructural evolution as a function of milling time. And then, the MMed powders were sintered by both spark plasma sintering and hot pressing in vacuum (HP). After the sintering process, MM-SPSed specimens were heat-treated in a vacuum furnace (SPS-VHT) and in the SPS equipment(MM-SPS) for microstructural control. It was found from microstrutural observation that the microstructure consisting of equiaxed ${gamma}$-TiAl with a few hundred nanometer in average size and ${alpha}_2-Ti_3Al$ particles were formed after both sintering processes. It was also revealed from hardness test and three-point bending test that the effect of grain refinement on the hardness and bending strength is much higher than that of carbon addition. The fully lamellar microstructures, which is less than $80{mu}m$ in average grain size was obtained by SPS-VHT process, and the fully lamellar microstructure which is less than $100{mu}m$ in average grain size was obtained by MM-SPS for a relatively shorter heat-treatment time.