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Preparation of Nano-sized Indium Tin Oxide (ITO) Powders and Their Sintering Behavior
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  • Preparation of Nano-sized Indium Tin Oxide (ITO) Powders and Their Sintering Behavior
  • Preparation of Nano-sized Indium Tin Oxide (ITO) Powders and Their Sintering Behavior
저자명
Lee. In-Gyu,Heo. Seung-Moo
간행물명
한국분말야금학회지
권/호정보
2004년|11권 6호|pp.467-471 (5 pages)
발행정보
한국분말야금학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

In order to fabricate a high density sintered body of ITO, nano-sized ITO powders were synthesized by coprecipitation methods. Aqueous solutions of indium and tin salts were mixed and coprecipitated by changing their pH. Coprecipitated ITO powders possessed 20-30 nm crystallite size and a relatively high BET value $(35m^{2}/g),$ however, aggregation of particles were occurred. Therefore, a novel recrystallization technique was applied in order to eliminate the aggregates. The recrystallized ITO material consists of a little bit larger needlelike crystals, $20nm{ imes}80nm$, and it possesses a higher BET value $(57m^{2}/g)$ compared to the plain coprecipitated material $(35m^{2}/g),$. Metastable phase formation and higher content of aggregated particles were observed in the coprecipitated materials. Densification was $95{\%};to;98{\%}$ complete after 5 hour sintering at $1500^{circ}C$ for the recrystallized powders while densities of the coprecipitated powders were below $75{\%}.$