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수소 확산화염에서 화염온도가 TiO2 나노입자의 합성에 미치는 영향
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  • 수소 확산화염에서 화염온도가 TiO2 나노입자의 합성에 미치는 영향
저자명
이교우,이승복,이종수,배귀남,Lee. Gyo Woo,Lee. Seung Bok,Lee. Jongsoo,Bae. Gwi-Nam
간행물명
大韓機械學會論文集. Transactions of the Korean society of mechanical engineers. B. B
권/호정보
2005년|29권 9호|pp.1013-1021 (9 pages)
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대한기계학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

In this work, $TiO_2$ nanoparticles were synthesized using a N2-diluted hydrogen coflow diffusion flame. The effects of flame temperature on the crystalline structure and the size of formed nanoparticles were investigated. The maximum centerline temperature of the flame ranged from 1,920K for $H_2-only$ flame to 863k for $81\%;N_2-diluted$ flame. The morphology and the crystal structure of $TiO_2$ nanoparticles were analyzed by a TEM and a XRD, respectively. The particle size distribution was also measured by using a scanning mobility particle size. (SMPS). The mean particle diameter was calculated from the TEM images depended on the flame temperature, having minimum at about 1,look. Based on the SMPS measurements, the mean particle diameter of $TiO_2$ nanoparticles at flame temperatures > 1,300K was smaller than that at flame temperatures < 1,300K. From the XRD analysis, it was evident that the anatase fraction increased with decreasing the flame temperature. The portion of anatase phase in $TiO_2$ nanoparticles might be greater than $80\%$ when the flame temperature was lower than 1,000K.