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Making of Tantalum Powder Using the Hunter Process
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  • Making of Tantalum Powder Using the Hunter Process
  • Making of Tantalum Powder Using the Hunter Process
저자명
Cho. Sung-Wook,Shim. Gunchoo,Park. Je-Shin,Kim. Joon-Su,Bae. In-Sung,Yoon. Jae-Sik,Jeong. Seong-Man
간행물명
Metals and materials international
권/호정보
2006년|12권 1호|pp.51-56 (6 pages)
발행정보
대한금속재료학회
파일정보
정기간행물|ENG|
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기타
이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Tantalum powder was made from potassium heptafluorotantalate $(K_2TaF_7)$ using sodium as a reductant based on the Hunter metallothermic reduction method. The apparatus for the experiment was designed and built specifically for the present study. The tantalum particle size greatly decreased as the reduction temperature decreased from 860 to $740^{circ}C$. The particle size was fairly uniform, varying from $2~3{mu}m$ to submicron sizes depending on the reaction temperature. Holding the reactants for more than 10 minutes after the completion of a sodium feeding caused irregular particle growth, thereby affecting particle size uniformity. It was found to be possible to agglomerate the powder to tens of micrometers in size by a vacuum heat treatment at $1350^{circ}C$. The formation of $Ta_2C$ during the heat treatment shows that care must be taken to prevent contamination from the furnace environment.