- 방전플라즈마 소결법으로 제작한 β-FeSi2 소결체의 고온 내산화성
- ㆍ 저자명
- 장세훈,홍지민,오익현,Chang. Se-Hun,Hong. Ji-Min,Oh. Ik-Hyun
- ㆍ 간행물명
- 한국재료학회지
- ㆍ 권/호정보
- 2007년|17권 3호|pp.132-136 (5 pages)
- ㆍ 발행정보
- 한국재료학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Oxidation resistance of sintered ${eta}-FeSi_{2}$ was investigated at intermediate temperature range in air atmosphere. Fully dense and porous bodies of ${eta}-FeSi_{2}$ samples were fabricated by using the Spark Plasma Sintering (SPS). They were annealed at $900^{circ}C$ for 5days to obtain ${eta}-FeSi_{2}$ phase. The bulk samples were oxidized at $800,;900;and;950^{circ}C$ in air atmosphere. The high temperature oxidation tests reveal that amorphous $SiO_{2}$ layer, similar to Si was formed and grew parabolically on ${eta}-FeSi_{2}$. Accelerated oxidation is not observed as well as cracks and grain boundary oxidation. Granular ${varepsilon}-FeSi$ was developed below the oxide layer as a result of oxidation of ${eta}-FeSi_{2}$. Oxidation resistance of sintered ${eta}-FeSi_{2}$ was excellent for high-temperature thermoelectric application.