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Characterization of Mechanical Alloying Processed Ti-Si-B Nanocomposite Consolidated by Spark Plasma Sintering
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  • Characterization of Mechanical Alloying Processed Ti-Si-B Nanocomposite Consolidated by Spark Plasma Sintering
  • Characterization of Mechanical Alloying Processed Ti-Si-B Nanocomposite Consolidated by Spark Plasma Sintering
저자명
Lee. Hyung-Bock,Kwon. In-Jong,Lee. Hyung-Jik,Han. Young-Hwan
간행물명
한국세라믹학회지
권/호정보
2008년|45권 12호|pp.815-820 (6 pages)
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한국세라믹학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

The microstructure and mechanical properties of $TiB_2/Si$ nanocomposites based on the Ti-Si-B system, consolidated by spark plasma sintering of mechanically alloyed activated nanopowders, have been characterized. Mechanical Alloying was carried out in a planetary ball mill for 180 min with 350 rev $min^{-1}$. The powders were pressed in vacuum at a pressure of 60 MPa, generating a maximum temperature in the graphite mould of $1400^{circ}C$. Analysis of the synthesized nanocomposites by SEM, XRD and TEM showed them to consist of $TiB_2$ second phase, sub-micron in size, with no third phase. Composites consolidated from powders mechanically alloyed from an initial elemental powder mix of 0.3 mol Si, 0.7 mol Ti, and 2.0 mol B achieved the best relative density (97%) and bending strength (774 MPa); the highest Vickers hardness of 14.7 GPa was achieved for the 0.1-0.9-2.0 mol starting composition.