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TFA-MOD법으로 제조된 다층 YBCO 박막의 미세구조 관찰
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  • TFA-MOD법으로 제조된 다층 YBCO 박막의 미세구조 관찰
  • Microstructural Observation of Multi-coated YBCO Films Prepared by TFA-MOD
저자명
장석헌,임준형,이창민,황수민,최준혁,심종현,주진호,김찬중,Jang. Seok-Hern,Lim. Jun-Hyung,Lee. Chang-Min,Hwang. Soo-Min,Choi. Jun-Hyuk,Shim. Jong-Hyun,Joo.
간행물명
Progress in superconductivity
권/호정보
2008년|9권 2호|pp.167-172 (6 pages)
발행정보
한국초전도학회
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기타
이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
서지반출

기타언어초록

We fabricated $YBa_2Cu_3O_{7-x}$(YBCO) films on (00l) $LaAlO_3$ substrates prepared by metal organic deposition(MOD) method using trifluoroacetate(TFA) solution. The films with various thicknesses were prepared by repeating the dip-coating and calcining processes. The effects of film thickness on phase formation, microstructures, and critical properties were evaluated by X-ray diffraction, scanning electron microscopy, and transmission electron microscopy. The microstructure and resultant critical current($I_C$) and critical current density($J_C$) varied remarkably with film thickness: The ($I_C$) value increased from 39 to 160 A/cm-width as the number of coatings increased from one to four, while the corresponding $J_C$ was measured to be in the range of $0.84-1.21;MA/cm^2$. Both the $I_C$ and $J_C$ decreased when an additional coating was applied due to microstructural degradation, indicating that the optimum thickness is in the range of $1.1-1.8;{mu}m$. The possible cause for the decrease in the $I_C$ and $J_C$ value for film thicker than $1.8;{mu}m$ include non-uniform thickness, increased surface roughness, and the poor formability of the YBCO phase and texture arising from the insufficient heat treatment time with respect to the increased thickness.