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HDH공정에 의한 티타늄 분말제조 및 소결특성
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  • HDH공정에 의한 티타늄 분말제조 및 소결특성
저자명
최정철,장세훈,차용훈,오익현,Choi. Jung-Chul,Chang. Se-Hun,Cha. Young-Hoon,Oh. Ik-Hyun
간행물명
한국재료학회지
권/호정보
2009년|19권 2호|pp.55-60 (6 pages)
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한국재료학회
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정기간행물|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

In this study, Ti powder was fabricated from Ti scrap by a hydrogenation-dehydrogenation (HDH) method. The Ti powders were compacted by Spark plasma sintering (SPS) and the microstructure and mechanical properties of the powders were investigated. A hydrogenation reaction of Ti scrap occurred at temperatures near $450^{circ}C$ with a sudden increase in the reaction temperature and a decrease in the pressure of the hydrogen gas as measured in a furnace during the hydrogenation process. In addition, a dehydrogenation process was carried out at $750^{circ}C$ for 2hrs in a vacuum of $10^{-4}torr$. The Ti powder sizes obtained by hydrogenation-dehydrogenation and mechanical milling processes were in the range of $1{sim}90{mu}m$ and $1{sim}100{mu}m$, respectively. To fabricate Ti compacts, Ti powders were sintered under an applied uniaxial punch pressure of 40 MPa at in a range of $900{sim}1200^{circ}C$ for 5 min. The relative density of a SPSed compact was 99.6% at $1100^{circ}C$, and the tensile strength decreased with an increase in the sintering temperature. However, the hardness increased as the sintering temperature increased.