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Gas Chromatography Residue Analysis of Bifenthrin in Pears Treated with 2% Wettable Powder
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  • Gas Chromatography Residue Analysis of Bifenthrin in Pears Treated with 2% Wettable Powder
  • Gas Chromatography Residue Analysis of Bifenthrin in Pears Treated with 2% Wettable Powder
저자명
Choi. Jeong-Heui,Liu. Xue,Kim. Hee-Kwon,Shim. Jae-Han
간행물명
Toxicological research
권/호정보
2009년|25권 1호|pp.41-45 (5 pages)
발행정보
한국독성학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
서지반출

기타언어초록

This study was conducted to monitor the level of bifenthrin residues in pear sprayed with 2% bifenthrin wettable powder (WP) at the recommended rate at four different schedules prior to harvest. The target analyte was extracted with acetone, partitioned into dichloromethane, and then purified by florisil chromatographic column. The residue determination was performed on a DB-5 capillary column using GC with electron capture detector (ECD). Linearity of this method was quite good ($r^2$ = 0.9951) in the concentration ranged from 0.2 mg/kg to 10 mg/kg. Recovery test was carried out at two concentration levels, 0.2 mg/kg and 1.0 mg/kg, in three replicates, and their rates were from 82.9% to 107.2%. No quantitative bifenthrin was detected in pear of all kinds of treatments including the treatment sprayed 4 times until 7 days before harvest. This sensitive and selective method can be used to monitor the trace residual amounts of bifenthrin in pear in a quite low concentration level.