The objective of this experimental study is to verify atomization characteristics of emulsified fuel. The emulsified fuel made of adding the ultrasonic energy is analyzed with atomization characteristics and chemicophysics. As water contents within emulsified fuel and needle angle increase, SMD, viscosity and surface tension were analyzed. By measuring the distribution percentage of hydrogen volume by $^1H$-NMR spectrum, the proportion of aromatics and paraffins is analyzed and compared each other. The results of study is as follows. First, as water contents within emulsified fuel and needle angle of nozzle increases, SMD increases. Second, for the distribution percentage of hydrogen volume, the distribution percentage of aromatics is about 10% and the rest portion is paraffins.