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Preparation of Selective Ion Adsorbent by Photo curing with Acrylic and Phosphoric Acid on Jute Yarn
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  • Preparation of Selective Ion Adsorbent by Photo curing with Acrylic and Phosphoric Acid on Jute Yarn
  • Preparation of Selective Ion Adsorbent by Photo curing with Acrylic and Phosphoric Acid on Jute Yarn
저자명
Al-Mamun. Md.,Khan. Mubarak A.,Khan. Ruhul A.,Zaman. Haydar U.,Saha. M.,Huque. S.M.F.
간행물명
Fibers and polymers
권/호정보
2010년|11권 6호|pp.832-837 (6 pages)
발행정보
한국섬유공학회
파일정보
정기간행물|ENG|
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

Jute yarns were cured with acrylic acid (AA) and phosphoric acid (PA) using UV radiation in order to prepare selective ion adsorbent. A series of formulations were prepared in methanol containing varying percentages of (10-70 %) of AA and 2 % photo-initiator (PI) (Darocur-4043). jute yarns were soaked in this formulation for various soaking times (10-30 min) and cured under UV radiation of different intensities (20-50 UV passes). Concentration of AA, soaking time and intensity of UV radiation were optimized based on polymer loading (PL). The maximum PL (21 %) was observed for 50 % AA solution for 20 min soaking time at 40 UV passes. Various formulations were prepared using 5-15 % (w/w) of phosphoric acid, 50 % AA and 2 % PI in methanol. Then jute yarns were soaked in this solution for 20 min and irradiated at 40th UV pass. The concentration of PA was again optimized for maximum PL. It was found that the formulation containing 10 % PA, 50 % AA, 38 % methanol and 2 % PI showed 70.95 % of PL. To investigate the adsorbent behavior, a 10 ppm $CuSO_4$ solution was prepared and then grafted yarns were soaked in the solutions for 30-300 min at different conditions. After withdrawing the yarns, the remaining copper in the solution were measured by atomic absorption spectrophotometer (AAS). It was revealed that copper was successfully removed by using the grafted jute yarns.