As the development of construction technology and new materials, building requirements has been varied gadually. Comfortable environment and serviceability of production activity and energy conservation are being dealt with very seriously. Recently localization of engineering technology of Power Plant, however, construction materials and domestic technology are being developed forcingly. According to above topics this thes is going to study roof waterproofing, thermal insulation and evaluate adiabatic performance and evaluation of properties of waterproofing materials and energy conservation. The results of studying and evaluating of roof waterproofing, thermal insulation and adiabatic performance of Power Plant are as follows. 1. Sheet waterproofing method is better than that of asphalt waterproofing method in that adaptability of wearhertight, thermal resistant, contraction and expansion. 2. It is required to replace polyurethane or ethylene used as thermal insulation with rock wool which is noncombustible materials. 3. It is recommended to usd outer insulation method than inner insulation method due to superioty of outer insulation method. Efficiency of insulation materials used in power plant is generally good except perlite mortar used in the power plant(YGN 1-2, GRI 1-2).