- 전자회절을 이용한 격자상수의 측정 정확도 향상
- ㆍ 저자명
- 이상길,송경,김진규,Lee. Sang-Gil,Song. Kyung,Kim. Jin-Gyu
- ㆍ 간행물명
- 한국현미경학회지
- ㆍ 권/호정보
- 2011년|41권 1호|pp.75-79 (5 pages)
- ㆍ 발행정보
- 한국현미경학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
For quantitative analysis of nano-crystal structure, we reported the accuracy improvement method of lattice parameters measured from electron diffraction. For calculation of Au lattice parameters used as a standard crystal structure, it was considered two different acquisition methods (detector and enegy-filter) and three different calculation methods (conventional, least-square and regression fit). As a result, the measurement reliability could be enhanced by using CCD camera which gives higher performance, while energy-filtering did not affect the improvement the camera constant accuracy. Also, the accuracy of lattice parameters could be improved up to $10^{-4}$ order by regression fitting with correction formula. Finally, it is expected that the combination of regression fitting and intensity extraction from energy-filtered precession electron diffraction gives a solution of quantitative structure analysis for unknown nano-crystals.