In the study, the sorption behaviors of three different cellulose fibers were investigated using heavy metal solutions(Pb(II) and Cd(II)). The sorption dose during the adsorption and desorption was measured using an inductively coupled plasma spectrometer. The initial sorption by cotton was greater than that of the other fibers, while the total adsorption dose of rayon was larger than that of the others. The desorption dose of heavy metal ions from the fiber was negligibly small, indicating that the ions are very strongly physic-ochemically attached to the fiber.