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SiC-ZrB2복합체의 특성에 미치는 SPS의 압력영향
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  • SiC-ZrB2복합체의 특성에 미치는 SPS의 압력영향
저자명
이정훈,진범수,신용덕,Lee. Jung-Hoon,Jin. Bm-Soo,Shin. Yong-Deok
간행물명
전기학회논문지= The Transactions of the Korean Institute of Electrical Engineers
권/호정보
2011년|60권 11호|pp.2083-2087 (5 pages)
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대한전기학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

The SiC-$ZrB_2$ composites were produced by subjecting a 40:60 vol.% mixture of zirconium diboride($ZrB_2$) powder and ${eta}$-silicon carbide (SiC) matrix to spark plasma sintering(SPS). Sintering was carried out for 60sec at $1400^{circ}C$ (designation as TP145 and TP146), $1500^{circ}C$(designation as TP155 and TP156) and uniaxial pressure 50MPa, 60MP under argon atmosphere. The physical, electrical, and mechanical properties of the SiC-$ZrB_2$ composites were examined. The relative density of TP145, TP146, TP155 and TP156 were 94.75%, 94.13%, 97.88% and 95.80%, respectively. Reactions between ${eeta}$-SiC and $ZrB_2$ were not observed via x-ray diffraction (hereafter, XRD) analysis. The flexural strength, 306.23MPa of TP156 was higher than that, 279.42MPa of TP146 at room temperature, but lower than that, 392.30MPa of TP155. The properties of a SiC-$ZrB_2$ composites through SPS under argon atmosphere were positive temperature coefficient resistance (hereafter, PTCR) in the range from $25^{circ}C$ to $500^{circ}C$. The electrical resistivities of TP145, TP146, TP155 and TP156 were $6.75{ imes}10^{-4}$, $7.22{ imes}10^{-4}$, $6.17{ imes}10^{-4}$ and $6.71{ imes}10^{-4}{Omega}{cdot}cm$ at $25^{circ}C$, respectively. The densification of a SiC-$ZrB_2$ composite through hot pressing depend on the sintering temperature and pressure. However, it is convinced that the densification of a SiC-$ZrB_2$ composite do not depend on sintering pressure under SPS.