In order to overcome the detection limit by the current nondestructive evaluation technology, a nonlinear resonant ultrasound spectroscopy(NRUS) technique was applied for detection of micro-scale cracks in a material. A down-shift of the resonance frequency and a variation of normalized amplitude of the resonance pattern were suggested as the nonlinear parameter for detection of micro-scale cracks in a materials. A natural-like crack were produced in a standard compact tension(CT) specimen by a low cycle fatigue test and the resonance patterns were acquired in each fatigue step. As the exciting voltage increases, a down-shift of resonance frequency were increases as well as the normalized amplitude decrease. This nonlinear effects were significant and even greater in the cracked specimen, but not observed in a intact specimen.