In this study, we have investigated the maximum smoke density and the initial stage smoke density in order to see the characteristics of smoke release of the architectural surface materials and the architectural adhesives, using smoke density chamber. As a result of the study, polyurethane foam showed the highest smoke density index, 206.55 within 10 min. In the case of the other samples, reinforced styrofoam was followed as 39.90, general styrofoam 33.73, and glass fiber 5.40, respectively. In the intial stage of a fire, it is forecasted actually to give hardship at the clear visibility. In the case of architectural adhesives, the highest ranking was those for windows and doors 509.64, stone 275.63, wood 232.25, tile 18.65, and styrofoam 6.44 were followed, respectively. This result is an early research to show characteristics of smoke release through experiment. However, it is meaningful that this study can be used as a basic for further study on architectural fire hazard prediction.