Low oxygen treatment and heating treatment are used to prevent insects in the field of food science. These eco-friendly control methods can be applied to biological control technique in conservation treatment of organic cultural properties. To evaluate material stability, low-oxygen treatment and low oxygen treatment are applied to wood, pigment, paper and textile that are related to historical wooden buildings. As a result, wood moisture content declined after low oxygen treatment. But decline rate is a little, so it can be expected to turn back original state as time passes. And test result on pigment, paper, textile of chrominance and strength of test materials are stable. But after heating treatment, pigments are separated.