- 무가압 분말 충전 성형법에 의해 제조된 Si 성형체의 반응 소결과 가스압 소결에 관한 연구
- ㆍ 저자명
- 박정현,강민수,백승수,염강섭
- ㆍ 간행물명
- 요업학회지
- ㆍ 권/호정보
- 1996년|33권 12호|pp.1414-1420 (7 pages)
- ㆍ 발행정보
- 한국세라믹학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
Using Si powder with average particle size of 8${mu}{ extrm}{m}$ Si compacts were formed by pressureless powder packing method. The compacts were reaction bonded at 1350, 140$0^{circ}C$ for 3~35 hrs under N2/H2 atmosphere and its microstructures were examined. Reaction bonded silicon nitrides showed nitridation of 90% and relative density of 88% After the impregnation of 5wt% MgO as sintering additive using aqueous solution of Mg nitrate the Si compacts were reaction bonded at 140$0^{circ}C$ for 15hrs. The reaction bonded bodies were gas pressure sintered at 180$0^{circ}C$ 190$0^{circ}C$ 200$0^{circ}C$ for 150, 300min. They showed relative density of 95% bending strength of 600MPa and fracture toughness of 6 MPa.m1/2