The noise . vibration characteristics of Hypoid gears which were made from three seperate materials(SCM, TSCM, SNCM) under the identical process were investigated for the sake of durability improvement of differential gear compatible with low level noise gear set. For this study, we developed a rig experimental equipment which can perform close noise.vibration experiment of differential gear. Consequently, we could analyze the noise.vibration characteristics of final reduction gear by materials, and also we observed changes in both metallic structure and hardness according to the materials of pinion gear. In addition to this, the correlation between the vibration of the differential gear and the interior noise of the passenger vehicles was proved by analyzing the results of rig vibration experiment and field noise test.