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SHS법을 이용한 복합분말(Al2O3-SiC) 제조시 TiO2첨가의 영향
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  • SHS법을 이용한 복합분말(Al2O3-SiC) 제조시 TiO2첨가의 영향
저자명
윤기석,양범석,이종현,원창환,Yun. Gi-Seok,Yang. Beom-Seok,Lee. Jong-Hyeon,Won. Chang-Hwan
간행물명
한국재료학회지
권/호정보
2002년|12권 1호|pp.48-53 (6 pages)
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한국재료학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

$Al_2O_3-SiC$ and $Al_2O_3-SiC$-TiC composite powders were prepared by SHS process using $SiO_2,;TiO_2$, Al and C as raw materials. Aluminum powder was used as reducing agent of $SiO_2,;TiO_2$ and activated charcoal was used as carbon source. In the preparations of $Al_2O_3-SiC$, the effect of the molar ratio in raw materials, compaction pressure, preheating temperature and atmosphere were investigated. The most important variable affecting the synthesis of $Al_2O_3-SiC$ was the molar ratio of carbon. Unreactants remained in the product among all conditions without compaction. The optimum condition in this reaction was $SiO_2$: Al: C=3: 5: 5.5, 80MPa compaction pressure under Preheating of $400^{circ}C$ with Ar atmosphere. However there remains cabon in the optimum condition. The effect of $TiO_2$ as additive was investigated in the preparations of $Al_2O_3-SiC$. As a result of $TiO_2$ addition, $Al_2O_3-SiC$-TiC composite powder was prepared. The $Al_2O_3$ powder showed an angular type with 8 to $15{mu}m$, and the particle size of SiC powder were 5~$10{mu}m$ and TiC powder were 2 to $5{mu}m$.