- SHS법을 이용한 복합분말(Al2O3-SiC) 제조시 TiO2첨가의 영향
- ㆍ 저자명
- 윤기석,양범석,이종현,원창환,Yun. Gi-Seok,Yang. Beom-Seok,Lee. Jong-Hyeon,Won. Chang-Hwan
- ㆍ 간행물명
- 한국재료학회지
- ㆍ 권/호정보
- 2002년|12권 1호|pp.48-53 (6 pages)
- ㆍ 발행정보
- 한국재료학회
- ㆍ 파일정보
- 정기간행물| PDF텍스트
- ㆍ 주제분야
- 기타
$Al_2O_3-SiC$ and $Al_2O_3-SiC$-TiC composite powders were prepared by SHS process using $SiO_2,;TiO_2$, Al and C as raw materials. Aluminum powder was used as reducing agent of $SiO_2,;TiO_2$ and activated charcoal was used as carbon source. In the preparations of $Al_2O_3-SiC$, the effect of the molar ratio in raw materials, compaction pressure, preheating temperature and atmosphere were investigated. The most important variable affecting the synthesis of $Al_2O_3-SiC$ was the molar ratio of carbon. Unreactants remained in the product among all conditions without compaction. The optimum condition in this reaction was $SiO_2$: Al: C=3: 5: 5.5, 80MPa compaction pressure under Preheating of $400^{circ}C$ with Ar atmosphere. However there remains cabon in the optimum condition. The effect of $TiO_2$ as additive was investigated in the preparations of $Al_2O_3-SiC$. As a result of $TiO_2$ addition, $Al_2O_3-SiC$-TiC composite powder was prepared. The $Al_2O_3$ powder showed an angular type with 8 to $15{mu}m$, and the particle size of SiC powder were 5~$10{mu}m$ and TiC powder were 2 to $5{mu}m$.