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양축 정렬된 니켈기판의 표면 산화반응 연구
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  • 양축 정렬된 니켈기판의 표면 산화반응 연구
  • A Study on the Surface Oxidation Behavior of Cube-textured Nickel Substrate
저자명
안지현,김병주,김재근,김호진,홍계원,이희균,유재무,Ahn. Ji-hyun,Kim. Byeong-Joo,Kim. Jae-Geun,Kim. Ho-Jin,Hong. Gye-Won,Lee. Hee-Gyoun,Yoo. Jai-Moo
간행물명
Progress in superconductivity
권/호정보
2005년|7권 1호|pp.58-63 (6 pages)
발행정보
한국초전도학회
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이 논문은 한국과학기술정보연구원과 논문 연계를 통해 무료로 제공되는 원문입니다.
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기타언어초록

We investigated the surface oxidation behavior of cube-textured polycrystalline nickel at various oxidation conditions. Cube-textured NiO film was formed on a cube-textured polycrystalline nickel regardless of oxidation conditions but different growth behavior of NiO crystals was observed depending on the oxidation conditions. The introduction of water vapor into $O_2$ did not affect the texture evolution, but rough and porous microstructure was developed. Microstructure of NiO film tends to be denser as the oxygen partial pressure increases. It is interesting that (111) peak of theta - two theta diffraction pattern started to get stronger in air atmosphere and (111) plane became the major texture in the substrate oxidized in high purity argon gas. Small amount of high index crystallographic plane NiO peak crystal was observed when $N_{2}O$ was used as an oxidant while only (200) plane crystal was formed in dry $O_2$ atmosphere. Flat and smooth surface was changed into rough faceted one when ramping rate to oxidation temperature was faster. The grain size of NiO was decreased when the oxygen partial pressure was low. It was also observed that the modification of nickel surface suppressed the development of (200) texture.